The Effect of Food-Simulating Liquids on Surface Features of Single-Shade Universal Composites: An In Vitro Study.

Objectives: This study aimed to investigate the microhardness, surface roughness, and field emission scanning electron microscopes (FE-SEM) images of three different single-shade composites (Essentia Universal, Omnichroma, and Vittra APS Unique) in food simulation liquids such as ethanol, citric acid, and distilled water. Materials and Methods: Three single-shade universal composites were selected for this study. For each composite resin group, 92 samples (5-mm diameter and 2-mm depth) were prepared in plexiglass molds (N = 276). Then, samples were separated into four groups randomly consisting of 23 samples each (10 for hardness, 10 for roughness, and 3 for FE-SEM analysis). Three groups were immersed in food-simulating liquids (FSL)-citric acid (0.02N), distilled water, and 75% ethanol stored in a glass at 37°C for the next 7 days to simulate a wet oral environment. Control samples were stored in an opaque-light-proof box at room temperature. After the conditioning period, roughness and microhardness were measured, and FE-SEM analysis was performed. For statistical analysis, the two-way analysis of variance and Tukey honestly significant difference tests were used to evaluate roughness and microhardness (P < 0.05). Results: There was a statistically significant difference between the composites in terms of roughness and hardness averages (P = 0.001; P < 0.05). Omnichroma showed the most surface changes in ethanol storage, whereas Vittra Unique showed the most surface changes in citric acid storage such as Essentia. Conclusion: FSL that mimic various oral environments affect single-shade universal resin composite restorations.

The Effect of Different Finishing and Polishing Systems on Surface Properties of New Flowable Bulk-fill Resin Composite.

AIM: The purpose of this research was to explore how various finishing and polishing techniques affect the surface roughness (Ra) and gloss of flowable bulk-fill injectable resin composite utilized for posterior teeth restoration, following exposure to a range of food-simulating liquids (FSLs) over three months. MATERIALS AND METHODS: This study comprised fifty-six disk specimens of G-aenial™ Bulk Injectable flowable resin composite which were created using a Teflon mold (10 × 4 mm). Two techniques of finishing and polishing (F/P) were employed: The two-step 3M™ Sof-Lex™ F/P spiral wheels system and the multiple-step 3M™ Sof-Lex™ XT finishing disks supplemented by the Ultradent Jiffy HiShine polisher cup system. The Ra and gloss of the prepared specimens were measured using an interference microscope system and Horiba gloss checker respectively, immediately post-finishing and polishing and then reassessed after three months in artificial saliva and Coca-Cola. RESULTS: The two-step system showed a statistically significant difference, exhibiting greater "surface roughness (Ra)" and lower "surface gloss (GU)" mean values compared to the multiple-step system under different storage conditions, particularly after 3 months of storage (p = 0.001). CONCLUSION: The multiple-step polishing system improved the "Ra" and "GU" of resin composite, suggesting their suitability for posterior resin composite restorations. Acidic media had a deleterious impact on the "Ra" and "GU" of resin composite restoration. CLINICAL SIGNIFICANCE: The quality of resin composite restorations can be significantly improved with the correct use of finishing and polishing systems, particularly in complex areas of posterior teeth restorations, leading to successful dental procedures.

Effect of Resin Coating on Surface Roughness and Microhardness of High Viscous Glass Ionomer Cements

ABSTRACT@#High viscous glass ionomer cement (HVGIC) was recently developed for atraumatic restorative treatment (ART). However, its moisture sensitivity remains a limitation thus protective coating application is recommended. This study investigated the effect of resin coating on the surface roughness and microhardness of two HVGICs (Riva Self Cure HVGIC [RV] and Equia® Forte Fil [EQ]) conditioned in food-simulating liquids (FSLs). Fifty standard disc-shaped samples were fabricated using customised stainless-steel mould (10 × 2 mm). Coating was applied on top surface of all samples and subsequently divided into five groups: air (control), distilled water, 0.02 N citric acid, heptane and 50% ethanol-water solution. The samples were conditioned in FSLs at 37°C for seven days. Subsequently, the surface roughness and microhardness of samples were measured using optical profilometry and microhardness tester, respectively. SEM analysis was done for qualitative observation of surface morphological changes. Data were analysed using one-way ANOVA, two-way ANOVA and posthoc Tukey’s test (α = 0.05). Interestingly, the results revealed that surface roughness was significantly influenced by FSLs immersion, presence of coating and the materials itself (p < 0.001). The lowest surface roughness was found on control coated samples: RV (50.98±4.25) nm and EQ (62.77±3.92) nm, while the highest values seen on uncoated surfaces in citric acid: RV (505.26±31.10) nm and EQ (350.33±15.36) nm. RV samples had the lowest microhardness of 54.97±2.48 Vickers hardness number (VHN) post-immersion in citric acid. In conclusion, with the exception of RV conditioned in heptane and ethanol, the uncoated HVGICs generally had higher surface roughness than the coated HVGICs. HVGICs conditioned in citric acid showed the most significant increase in surface roughness and reduction in microhardness.

Effect of Dietary Challenges on the Flexural Properties of Resin-based Composites

@#This study aims to compare flexural strength and flexural modulus of different resin-based composites (RBCs) and to determine the impact of dietary solvents on flexural properties. Forty specimens (12x2x2mm) for each of two conventional (Aura Easy [AE]; Harmonize [HN]) and one bulk fill (Sonic Fill 2 [SF2]) were fabricated using customised plastic moulds. Specimens were light-cured, measured and randomly divided into four groups. The groups (n=10) were conditioned for 7 days at 37°C: in one of media: air (control), artificial saliva (SAGF), 0.02N citric acid and 50% ethanol–water solution. After conditioning, the specimens subjected to flexural testing. Two-way ANOVA and one-way ANOVA (post hoc: Tukey’s or Dunnett T3 tests) were used at =0.05. Significant differences in flexural properties were observed between materials and conditioning media. Flexural strength and modulus values ranged from 124.85MPa to 51.25MPa; and 6.76GPa to 4.03GPa, respectively. The highest flexural properties were obtained with conditioning in air. Exposure to aqueous solutions generally reduced flexural properties. In conclusion, the effect of dietary solvents on flexural properties were material and medium dependent. For functional longevity of restorations, patients’ alcohol intake should be considered during material selection. Dietary advice (reduce alcohol consumption) should be given to patients post operatively.

Chemical degradation of dental CAD/CAM materials.

BACKGROUND: The chemical properties of the oral environment have an appreciable influence on the in vivo degradation of CAD/CAM materials. OBJECTIVE: The aim of the present study was to investigate the effect of organic acids, heptane and ethanol (the food-simulating liquids) on CAD/CAM restorative materials. METHODS: Four CAD/CAM materials were selected: (1) 3M ESPE LAVA Ultimate, (2) VITA Enamic, (3) IPS e.max CAD, (4) VITA Suprinity. Seven different samples were fabricated in 15 × 4 × 1.2 mm dimensions from each material (n = 7, N = 140). The materials were conditioned for 7 days at 37 °C as follows: artificial saliva, 75% ethanol, heptane, 0.02 N citric acid, 0.02 N lactic acid in aqueous solution and were tested to obtain flexural strength, surface micro-hardness and wear characteristics. After conditioning, the flexural strength values were assessed using a universal testing machine (1 mm/min crosshead speed) and the fractured samples were used for determination of Vickers hardness values using a digital micro-hardness tester (100 g/10 s) and determination of wear using a chewing simulator. Two factor analysis of variance with interaction model and Tukey's post hoc test were used for statistical analysis. RESULTS: The highest mechanical property values were found for IPS e.max and VITA Suprinity and the lowest values were found for LAVA Ultimate. Organic acids negatively affected the mechanical properties of e.max CAD and Suprinity. Ethanol and heptane were more effective on LAVA Ultimate and Enamic. There were significant differences among groups (p < 0.05). CONCLUSION: The mechanical properties of CAD/CAM restorative materials are influenced by food-simulating liquids.

Comparison of the Water Sorption and Solubility of Four Reline Acrylic Resins after Immersion in Food-Simulating Agents.

OBJECTIVES: Water sorption and water solubility adversely affect the mechanical properties and biocompatibility of the denture material. This study aimed to evaluate the water sorption and solubility of three direct hard reline acrylic resins and a heat-curing one after immersion in food-simulating agents. MATERIALS AND METHODS: This study was performed on four groups of samples (n = 10 per group). The samples were made of three direct hard reline acrylic resins (TDV Cold Liner Rebase, Tokuyama Rebase II Fast, GC Reline Hard) and a heat-curing one (Meliodent). Each group was divided into four subgroups (n = 10) to undergo 7-day immersion in distilled water, 75% ethanol/water, 0.02 N citric acid, and heptane. Water sorption and solubility were calculated according to Oysaed and Ruyter formula. The statistical analyses were done by using SPSS software (version 22). Kruskal-Wallis H Test and Dunn's test were used to detect any significant difference among the groups (P < 0.05). RESULTS: The median range of water solubility and water sorption values were -0.87-4.92 and 3.75-27.25 µg/mm3, respectively. The median solubility and sorption values of different resins differed significantly in the same solution (P < 0.05). Besides, immersion in different solutions caused significant differences in the median solubility and sorption values of each reline material (P < 0.05), except for Meliodent whose solubility was not significantly affected by different solutions (P = 0.16). CONCLUSIONS: Water sorption and solubility values of the tested hard reline resins were within the range of International Standards Organization 1567:1999. Given the low sorption and solubility values, these hard reline materials can be safely used in clinical situations.