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1.
ACS Appl Mater Interfaces ; 16(22): 28780-28790, 2024 Jun 05.
Artigo em Inglês | MEDLINE | ID: mdl-38771252

RESUMO

Developing a simple and rapidly preparative method for patterned flexible supercapacitors is essential and indispensable for the swift advancement of portable devices integrated with micro devices. In this study, we employed a cost-effective and rapid fabrication method based on transfer-printing technology to produce patterned micro flexible supercapacitors with various substrates. The resulting flexible micro supercapacitors not only allow for customized patterns with strong flexibility and resistance to bending, while maintaining a certain level of performance, but also facilitate the creation of diverse circuits to tailor voltage and current to specific requirements. Patterned micro flexible supercapacitors with a thickness of 0.02 mm, based on accordion-like Ti3C2Tx MXene materials coated on a substrate, demonstrate a specific capacitance of 142.7 mF cm-2 at 0.5 mA cm-2. The devices exhibit satisfactory capacitance retention (91% after 5000 cycles) and superb mechanical flexibility (71% capacitance retention at 180° bending after 2000 cycles). At a power density of 2.9 mW cm-2, the energy density of the sandwich structure device reaches 126.8 µWh cm-2. This study is expected to contribute new ideas for the design and preparation of patterned flexible supercapacitors.

2.
Adv Mater ; : e2402695, 2024 May 14.
Artigo em Inglês | MEDLINE | ID: mdl-38742820

RESUMO

Flexible supercapacitors can potentially power next-generation flexible electronics. However, the mechanical and electrochemical stability of flexible supercapacitors under different flexible conditions is limited by the weak bonding between adjacent layers, posing a significant hindrance to their practical applicability. Herein, based on the uninterrupted 3D network during the growth of bacterial cellulose (BC), a flexible all-in-one supercapacitor is cultivated through a continuous biosynthesis process. This strategy ensures the continuity of the 3D network of BC throughout the material, thereby forming a continuous electrode-separator-electrode structure. Benefitting from this bioinspired structure, the all-in-one supercapacitor not only achieves a high areal capacitance (3.79 F cm-2) of electrodes but also demonstrates the integration of high tensile strength (2.15 MPa), high shear strength (more than 54.6 kPa), and high bending resistance, indicating a novel pathway toward high-performance flexible power sources.

3.
Heliyon ; 9(11): e21799, 2023 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-38034807

RESUMO

Efficient thermal insulation materials considerably lower power consumption for heating and cooling of buildings, which in turn minimises CO2 emissions and improves indoor comfort conditions. However, the selection of suitable insulation materials is governed by several factors, such as the environmental impact, health impact, cost and durability. Additionally, the disposal of used insulation materials is a major factor that affects the selection of materials because some materials could be very toxic for humans and the environment, such as asbestos-containing materials. Therefore, there is a continuous research effort, in both industry and academia, to develop sustainable and affordable insulation materials. In this context, this work aims at utilising the packing industry wastes (cardboard) to develop an eco-friendly insulation layer, which is a biodegradable material that can be disposed of safely after use. Experimentally, wasted cardboard was collected, cleaned, and soaked in water for 24 h. Then, the wet cardboard was minced and converted into past papers, then cast in square moulds and left in a ventilated oven at 75 °C to dry before de-moulding them. The produced layers were subjected to a wide range of tests, including thermal conductivity, acoustic insulation, infrared imaging and bending resistance. The obtained results showed the developed material has a good thermal and acoustic insulation performance. Thermally, the developed material had the lowest thermal conductivity (λ) (0.039 W/m.K) compared to the studied traditional materials. Additionally, it successfully decreased the noise level from 80 to about 58 dB, which was better than the efficiency of the commercial polyisocyanurate layer. However, the bending strength of the developed material was a major drawback because the material did not resist more than 0.6 MPa compared to 2.0 MPa for the commercial polyisocyanurate and 70.0 MPa for the wood boards. Therefore, it is recommended to investigate the possibility of strengthening the new material by adding fibres or cementitious materials.

4.
Materials (Basel) ; 16(14)2023 Jul 19.
Artigo em Inglês | MEDLINE | ID: mdl-37512354

RESUMO

How to effectively reinforce steel structures with rust and damage is an important research topic in the engineering field. This article takes the rusted I-beam as the research object and analyzes the effects of different CFRP/GFRP reinforcement methods on the bending performance of rusted I-beams through experimental research with a total of 1 unreinforced beam and 7 CFRP/GFRP-reinforced beams. The results show that when the number of CFRP/GFRP-reinforced layers is the same, replacing some of the CFRP with GFRP and using different interlayer mixed laying sequences have little effect on the bending bearing capacity of rusted I-beams. The number of CFRP/GFRP-reinforced layers is the key factor affecting the bending bearing capacity. At the same time, numerical simulation was conducted using finite element software to study the stress distribution and stress development law of the reinforced beam, and the numerical simulation results were consistent with the experimental results.

5.
Materials (Basel) ; 16(7)2023 Mar 30.
Artigo em Inglês | MEDLINE | ID: mdl-37049070

RESUMO

Damage often develops in glued laminated timber members under high bending loads due to natural defects in the timber, which results in their low load-bearing capacity and stiffness. In order to improve the bending mechanical properties of glulam beams, a new type of longitudinal glulam reinforcement with pre-stressed basalt fibre-reinforced polymer composites (BFRP) was developed using the Near Surface Mounted (NSM) technique. The strengthening method consisted of two pre-stressed BFRP bars glued into the grooves at the bottom side of the beam; meanwhile, for the second strengthening alternative, the third BFRP bar was embedded into the groove at the top side of the beam. Therefore, an experimental study was carried out to verify this strengthening technique, in which fifteen full-size timber beams were tested with and without bonded BFRP bar reinforcement in three series. According to the results of this experimental study, it can be seen that the effective load-bearing capacity of the reinforced beams increased up to 36% and that the stiffness of the beams increased by 23% compared to the unreinforced beams. The tensile stresses in the wooden fibres were reduced by 11.32% and 25.42% on average for the beams reinforced with two and three BFRP bars, respectively. On the other hand, the compressive stresses were reduced by 16.53% and 32.10% compared to the unreinforced beams. The usual failure mode saw the cracking of the wood fibres at the defects, while for some specimens, there were also signs of cracks in the epoxy adhesive bond; however, the crack propagation was, overall, significantly reduced. The numerical calculations also show a good correlation with the experimental results. The difference in the results between the experimental and numerical analysis of the reinforced and unreinforced full-sized beams ranged between 3.63% and 11.45%.

6.
Materials (Basel) ; 16(2)2023 Jan 16.
Artigo em Inglês | MEDLINE | ID: mdl-36676616

RESUMO

To investigate the normal section strength and cracking bending moment of normal concrete-ultra-high-performance concrete (NC-UHPC) composite beams, calculation formulas were established considering the tensile strength of UHPC based on the current railway bridge design code. Using the railway T-beam as a template, prestressed NC-UHPC composite beams with different NC layer heights were built. A static bending test was performed, the pressure of the steel strand and the deflection and strain of the beam were measured, and the evolution of cracks in each beam was observed. The calculation formulas of the normal section strength and cracking bending moment of NC-UHPC composite beam were verified by the test. The results showed that the type of strain was similar to load-deflection curves with increasing load; the bending failure process of the NC-UHPC composite beam showed four obvious stages: elasticity, uniform cracking, crack development, and yield. Cracks in the beam started to appear at stage II, developed rapidly at stage III, and stopped emerging at stage IV. The calculation formulas for the normal section strength and the cracking bending moment of the NC-UHPC composite beam were in good agreement with the test values. Normal concrete with a compressive strength of 80 MPa can replace UHPC for the design of NC-UHPC composite beams.

7.
J Endod ; 49(3): 301-306, 2023 Mar.
Artigo em Inglês | MEDLINE | ID: mdl-36567061

RESUMO

INTRODUCTION: The aim of this study was to compare E1-Irrisonic (Helse Ultrasonics, Ocoee, FL) and Irri Black (Helse Ultrasonics), a novel ultrasonic tip with diamondlike carbon treatment, regarding their design, metallurgy, microhardness, bending resistance, and time to fracture under the oscillatory fatigue test. METHODS: A total of 17 E1-Irrisonic and 17 Irri Black new ultrasonic tips were selected. The tip geometry and surface finishing were assessed using scanning electron microscopy. The elemental composition was defined by energy-dispersive X-ray spectroscopy. Hardness Knoop was calculated using a microhardness tester. The maximum load required to displace the instrument in 45° was recorded in gram/force, oscillatory fatigue was measured in seconds at the moment of instrument fracture, and the size of the separate fragments was determined in millimeters. The Student t test was used for statistical comparison (α = 5%). RESULTS: Scanning electron microscopic analyses revealed that E1-Irrisonic had a flat end tip, whereas a noncutting rounded tip was observed in Irri Black. The surface of E1-Irrisonic was smoother than Irri Black, which was irregular. Energy-dispersive X-ray spectroscopic analyses showed that the elemental compositions of the E1-Irrisonic and Irri Black tips were consistent with stainless steel and titanium-aluminum alloys, respectively. Irri Black showed significantly higher bending load resistance, time to fracture under oscillatory motion, and hardness Knoop than the E1-Irrisonic tip (P < .05), whereas the length of fragments was similar (P > .05). CONCLUSION: Diamondlike carbon treatment improved hardness Knoop and reduced the flexibility of the Irri Black ultrasonic tip, improving its time to fracture under oscillatory motion compared with the nontreated E1-Irrisonic tip.


Assuntos
Carbono , Ultrassom , Humanos , Dureza , Titânio/química , Teste de Materiais , Microscopia Eletrônica de Varredura , Propriedades de Superfície , Desenho de Equipamento , Preparo de Canal Radicular
8.
Nanomicro Lett ; 15(1): 25, 2022 Dec 30.
Artigo em Inglês | MEDLINE | ID: mdl-36583830

RESUMO

Covalent organic framework (COF) film with highly exposed active sites is considered as the promising flexible self-supported electrode for in-plane micro-supercapacitor (MSC). Superlattice configuration assembled alternately by different nanofilms based on van der Waals force can integrate the advantages of each isolated layer to exhibit unexpected performances as MSC film electrodes, which may be a novel option to ensure energy output. Herein, a mesoporous free-standing A-COF nanofilm (pore size is 3.9 nm, averaged thickness is 4.1 nm) with imine bond linkage and a microporous B-COF nanofilm (pore size is 1.5 nm, averaged thickness is 9.3 nm) with ß-keto-enamine-linkages are prepared, and for the first time, we assembly the two lattice matching films into sandwich-type superlattices via layer-by-layer transfer, in which ABA-COF superlattice stacking into a "nano-hourglass" steric configuration that can accelerate the dynamic charge transportation/accumulation and promote the sufficient redox reactions to energy storage. The fabricated flexible MSC-ABA-COF exhibits the highest intrinsic CV of 927.9 F cm-3 at 10 mV s-1 than reported two-dimensional alloy, graphite-like carbon and undoped COF-based MSC devices so far, and shows a bending-resistant energy density of 63.2 mWh cm-3 even after high-angle and repeat arbitrary bending from 0 to 180°. This work provides a feasible way to meet the demand for future miniaturization and wearable electronics.

9.
Materials (Basel) ; 15(9)2022 May 06.
Artigo em Inglês | MEDLINE | ID: mdl-35591664

RESUMO

This study aimed to evaluate and compare the dynamic cyclic fatigue, torsional and bending resistance of two novel RACE EVO (FKG Dentaire SA, La Chaux de Fonds, Switzerland) and R-Motion (FKG) nickel−titanium instruments with traditional RaCe (FKG) instruments. RACE EVO, R-Motion and RaCe instruments with a size of 25 and taper of 0.06 were used. A dynamic cyclic fatigue test was used to assess the time to fracture. The fractured surfaces were further analyzed using scanning electron microscopy at ×350 and ×3000 magnifications. A torsional resistance test was performed to measure the maximum torsional strength and angle of rotation. Phase transformations with temperature were evaluated using differential scanning calorimetry. The results were statistically analyzed with a Kruskal−Wallis test at a 5% significance level. R-Motion had the highest time to fracture and the lowest torsional and bending resistance, whereas RaCe had the lowest time to fracture and the highest torsional and bending resistance (p < 0.05). In relation to the angle of rotation, RACE EVO instruments had the highest deformation capacity followed by R-Motion and RaCe instruments (p < 0.05). The greater cyclic fatigue resistance and lower torsional and bending resistance results indicate that the novel R-Motion and RACE EVO instruments are less rigid and more flexible than RaCe instruments.

10.
Int Endod J ; 53(12): 1689-1695, 2020 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-32767775

RESUMO

AIM: To evaluate the bending, buckling and torsional resistance of ProGlider (PG) (Dentsply Sirona, Ballaigues, Switzerland), R-Pilot (RP) (VDW, Munich, Germany) and WaveOne Gold Glider (WOGG) (Dentsply Sirona). METHODOLOGY: Ninety instruments were used: 30 PG (size 0.16, .02v taper), 30 RP (size 0.125, .04 taper) and 30 WOGG (size 0.15, .02v taper). The bending resistance test was performed on 10 randomly selected instruments of each system according to ISO 3630-1 specifications. For the buckling resistance test, a loading was applied in the axial direction of each instrument using a universal test machine, with a 20 N cell and 15 mm min-1 speed, in the axial direction. When a lateral elastic displacement of 1 mm occurred, the force was registered. The torsional resistance test was performed according to ISO 3630-1 specifications. Statistical analysis was performed using one-way anova and post hoc Student-Newman-Keuls test (P < 0.05). RESULTS: WOGG had the lowest bending resistance, whilst RP had the highest bending resistance (P < 0.05). RP also had the highest buckling resistance, and WOGG had the lowest (P < 0.05). PG had intermediate results regarding bending and buckling resistance, with significant differences to RP and WOGG (P < 0.05). RP had the highest torsional strength and the lowest angular deflection when compared to PG and WOGG (P < 0.05). No differences in the torsional strength and angular deflection were observed between WOGG and PG (P> 0.05). CONCLUSION: The glide path instruments had different behaviours in term of bending, buckling and torsional resistance.


Assuntos
Instrumentos Odontológicos , Fenômenos Mecânicos , Ligas Dentárias , Desenho de Equipamento , Alemanha , Ouro , Humanos , Teste de Materiais , Preparo de Canal Radicular , Titânio , Torção Mecânica
11.
J Dent Sci ; 15(4): 472-478, 2020 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-33505619

RESUMO

BACKGROUND/PURPOSE: Several single-file systems manufactured using different heat treatment and operated by different kinematics have been released. This study compared the bending resistance and cyclic fatigue resistance of three NiTi files, and examined their phase-transformation behavior. MATERIALS AND METHODS: WaveOne Gold Primary (WOG), Reciproc Blue R25 (RPB), and HyFlex EDM OneFile (HDM) were tested (N = 40/instrument). A vertical load was applied to a point 3 mm from the tip, and the stress was measured until a displacement of 3 mm. Tests were conducted at either room temperature (RT: 22 °C) or body temperature (BT: 37 °C) (n = 10). Cyclic fatigue resistance tests were performed in an artificial canal, which had a curvature angle of 40° and a 5-mm radius. Tests were conducted at either RT or BT (n = 10). Instruments were operated according to the manufacturers' instructions. Test results were analyzed using the Kruskal-Wallis and the Mann-Whitney tests. Additional three instruments of each brand were subjected to differential scanning calorimetry (DSC). RESULTS: At RT the bending resistance of three files were not significantly different. However, at BT the bending resistance of RPB was highest, followed by WOG, and HDM (P < 0.05). At RT, RPB demonstrated the longest fracture time, followed by HDM, and WOG (P < 0.05). At BT, HDM had the longest fracture time, followed by RPB, and WOG (P < 0.05). The WOG, RPB consisted of austenite in a considerable proportion, whereas HDM was mainly martensite state at BT. CONCLUSION: HDM presented superior flexibility and cyclic fatigue resistance at BT.

12.
J Mech Behav Biomed Mater ; 90: 165-172, 2019 02.
Artigo em Inglês | MEDLINE | ID: mdl-30366307

RESUMO

To evaluate the bending and torsional properties of four nickel-titanium endodontic files, we simulated and compared WaveOne® primary size 25 with 0.07 taper, WaveOne Gold® primary size 25 with 0.07 taper, Reciproc® primary size 25 with 0.08 taper, and Reciproc Blue® primary size 25 with 0.08 taper. Three-dimensional models were created using computer-aided design software and numerically analyzed in ANSYS® Workbench. Boundary conditions for the numerical analyses were based on the ISO 3630-1 specifications. The highest stress levels were recorded for WaveOne® and Reciproc®. Numerical results of the bending test showed that WaveOne Gold® is 86% more flexible than WaveOne® with a deflection of 3 mm. Reciproc Blue® was 42.31% more flexible than Reciproc® file with a deflection of 3 mm. The WaveOne® instrument withstood the highest stress under the torsion test, followed by Reciproc®, then Reciproc Blue® files. The stress under torsion in the WaveOne® and WaveOne Gold® files is reduced in a 51%. Regarding Reciproc® and Reciproc Blue® files, the stress under torsional moments remains very similar. Our results exposed a considerable difference in terms of stress tolerance between WaveOne® and WaveOne Gold®. However, Reciproc® files demonstrated a similar stress distribution. The results obtained through finite element analysis suggest that thermal treatment of files might improve their flexibility, increasing resistance during the preparation of highly curved canals. Also, the values obtained regarding the improvement of flexibility were in accordance with the manufacturer claims.


Assuntos
Ligas Dentárias , Endodontia , Análise de Elementos Finitos , Teste de Materiais , Fenômenos Mecânicos , Níquel , Titânio
13.
ACS Appl Mater Interfaces ; 10(10): 8917-8925, 2018 Mar 14.
Artigo em Inglês | MEDLINE | ID: mdl-29457446

RESUMO

Flexible transparent electrodes are an indispensable component for flexible optoelectronic devices. In this work, the meter-scale composite transparent electrodes (CTEs) composed of poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and Ag grid/polyethylene terephthalate (PET) with optimized mechanical and optical properties are demonstrated by slot-die roll-to-roll technique with solution printing method under a low cost ($15-20 per square meter), via control of the viscosity and surface energy of PEDOT:PSS ink as well as the printing parameters. The CTEs show excellent flexibility remaining 98% of the pristine value after bending 2000 times under various bending situations, and the square resistance ( Rs) of CTEs can be reduced to 4.5-5.0 Ω/sq with an appropriate transmittance. Moreover, the optical performances, such as haze, extinction coefficient, and refractive index, are investigated, as compared with indium tin oxide/PET, which are potential for the inexpensive optoelectronic flexible devices. The CTEs could be successfully employed in polymer solar cells with different areas, showing a maximal power conversion efficiency of 8.08%.

14.
Int Endod J ; 51(9): 1047-1052, 2018 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-29478247

RESUMO

AIM: To compare the cyclic fatigue resistance and bending properties of R-Pilot and WaveOne Gold (WOG) Glider files, at intracanal temperature (35°C). METHODOLOGY: Forty R-Pilot and 40 WOG Glider files were subjected to a cyclic fatigue resistance test (n = 20), calculating the time to fracture (TTF) in an artificial stainless steel canal. The length of the fractured file tips (FL) was also measured. The fracture surface of fragments was examined with a scanning electron microscope, and the cross-sectional area of the fractured surfaces was measured. Flexibility of the tested files (n = 20) was determined using 45° bending test. Data were analysed statistically using the Mann-Whitney U-test at 5% significance level. RESULTS: Time to fracture was significantly higher in the R-Pilot group compared to the WOG Glider (P < 0.05). There was no significant difference between groups for fracture length. The bending resistance of R-Pilot files was significantly greater than WOG Glider files (P < 0.05). CONCLUSIONS: A significant greater cyclic fatigue resistance was observed for R-Pilot files compared to WOG Glider instruments, although the bending resistance of WOG Glider files was lower.


Assuntos
Obturação do Canal Radicular/instrumentação , Ligas , Cavidade Pulpar/cirurgia , Falha de Equipamento , Análise de Falha de Equipamento , Humanos , Microscopia Eletrônica de Varredura
15.
Int Endod J ; 50(11): 1077-1083, 2017 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-27917513

RESUMO

AIM: To compare the torsional and bending resistance of WaveOne Gold (Dentsply Tulsa Dental Specialties, Tulsa, OK, USA), Reciproc (VDW, Munich, Germany) and Twisted File Adaptive (Axis/SybronEndo, Orange, CA, USA) instruments. METHODOLOGY: Torsional strength of WaveOne Gold primary size 25, .07 taper, Reciproc size 25, .08 taper and Twisted File Adaptive M-L1 size 25, .08 taper was measured by fastening the apical 3 mm of the instrument firmly and applying a constant rotation at 2 rpm to the instrument using a torsiometer. The fractured instruments were examined using a scanning electron microscope (SEM). The bending resistance of the instruments was measured using the cantilever bending test. The data were statistically analysed using one-way analysis of variance (anova) and Tukey post hoc tests. The statistical significance level was set at P < 0.05. RESULTS: WaveOne Gold had a significantly higher torsional resistance than Reciproc and Twisted File Adaptive (P < 0.001). Reciproc had a significantly higher torsional resistance than Twisted File Adaptive (P < 0.001). WaveOne Gold had a significantly lower resistance to bend than Reciproc and Twisted File Adaptive (P < 0.001). There was a significant difference in bending resistance between Reciproc and Twisted File Adaptive instruments (P < 0.001). SEM of the fracture cross-sectional surface displayed the classical features of torsional failure, including fibrous dimple marks near the centre of rotation and circular abrasion marks. CONCLUSIONS: WaveOne Gold exhibited higher resistance to torsional stress and flexibility compared with Reciproc and Twisted File Adaptive instruments. Torsional resistance and flexibility properties of the instruments could be affected by the alloy from which the instrument is manufactured and different cross-sectional design.


Assuntos
Instrumentos Odontológicos/normas , Análise de Variância , Torção Mecânica
16.
J Endod ; 42(12): 1789-1793, 2016 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-27776886

RESUMO

INTRODUCTION: This study evaluated the bending resistance and cyclic fatigue life of a new single-file reciprocating instrument (Unicone; Medin, Nové Mesto na Morave, Czech Republic). Reciproc (VDW, Munich, Germany) and WaveOne (Dentsply Maillefer) instruments were used as references for comparison. METHODS: Flexibility was determined by 45° bending tests using a universal testing machine. The cyclic fatigue test was performed using a custom-made device. For this test, an artificial canal with a 60° angle and a 5-mm radius of curvature was used. Scanning electron microscopic analysis was performed to determine the mode of fracture and possible deformations at the helical shaft. Statistical analysis for the bending resistance test was performed using parametric methods (ie, 1-way analysis of variance). Post hoc pair-wise comparisons were performed using the Tukey test for multiple comparisons (P < .05). Weibull analysis was used to calculate the mean life, beta, and eta parameters. RESULTS: Reciproc presented significantly lower bending resistance than the other tested systems (P < .05), whereas no differences were observed between WaveOne and Unicone (P > .05). When mean life was compared among the brands, Reciproc lasted longer than WaveOne with a probability of 99.9%, longer than Unicone in the "RECIPROC ALL" mode with a probability of 99.9%, and longer than Unicone in the "WAVEONE ALL" mode with a probability of 99.9% (all statistically significant). Moreover, WaveOne lasted longer than Unicone in the "RECIPROC ALL" mode with a probability of 98.5% and longer than Unicone in the "WAVEONE ALL" mode with a probability of 99.8% (all statistically significant). Finally, Unicone in the "RECIPROC ALL" mode lasted longer than Unicone in the "WAVEONE ALL" mode with a probability of 95.3% (statistically significant). CONCLUSIONS: The new reciprocating instrument Unicone showed lower cyclic fatigue resistance compared with Reciproc R25 and WaveOne Primary files.


Assuntos
Ligas Dentárias/química , Desenho de Equipamento , Níquel/química , Preparo de Canal Radicular/instrumentação , Titânio/química , Instrumentos Odontológicos , Análise do Estresse Dentário/instrumentação , Falha de Equipamento , Teste de Materiais , Microscopia Eletrônica de Varredura , Maleabilidade , Distribuição Aleatória , Rotação , Aço Inoxidável/química , Estresse Mecânico , Propriedades de Superfície
17.
Eur Endod J ; 1(1): 1-4, 2016.
Artigo em Inglês | MEDLINE | ID: mdl-32566901

RESUMO

OBJECTIVE: The present study aimed to evaluate the bending resistance and cyclic fatigue fracture resistance of a new single-file reciprocating instrument called WaveOne Gold. Reciproc and WaveOne instruments were used as references for comparison. METHODS: Sixty 25-mm NiTi instruments (Reciproc R25, WaveOne Primary and WaveOne Gold Primary) were tested. Flexibility was determined by applying 45° bending tests using a universal testing machine (n=10). A custom-made device was used during cyclic fatigue test (n=10), comprising a stainless steel artificial canal measuring 1.4 mm in diameter, 19 mm in total length with an 86° angle and 6 mm radius of curvature. Possible deformations at the helical shaft and mode of fracture were evaluated using scanning electron microscopy analysis. Statistical analysis was performed using one-way analysis of variance. Post hoc pair-wise comparisons were performed using Tukey's test for multiple comparisons (P<0.05). RESULTS: WaveOne presented significantly higher bending resistance than the other tested systems (P<0.05), whereas Reciproc presented the lowest bending resistance (P<0.05). Reciproc revealed a significantly longer cyclic fatigue fracture resistance than the other systems (P<0.05). CONCLUSION: Although WaveOne Gold presented higher flexibility than WaveOne, no differences in the resistance to fatigue were observed between both systems. The Reciproc files were more flexible and resistant to fatigue for the angle of curvature of 86° and 6 mm radius than WaveOne and WaveOne Gold files.

18.
Rev. bras. odontol ; 69(2): 170-173, Jul.-Dez. 2012. tab
Artigo em Português | LILACS | ID: lil-720334

RESUMO

Esse estudo avaliou e comparou a resistência em flexão de instrumentos endodônticos mecanizados obtidos de fios metálicos de níquel-titânio (NiTi) convencional e M-wire. Para avaliar a resistência em flexão empregou-se o ensaio mecânico de flexão em cantilever. A flexibilidade em flexão de um instrumento endodôntico depende da composição química e do tratamento termomecânico da liga metálica, assim como, da geometria da seção reta transversal da haste cônica helicoidal do instrumento endodôntico. Os resultados obtidos revelaram que os instrumentos Profile Vortex, fabricados a partir de fios metálicos de NiTi denominados M-wire, apresentaram a maior resistência em flexão (menor flexibilidade). Os instrumentos RaCe, produzidos a partir de fios metálicos de NiTi convencional, apresentaram a menor resistência em flexão (maior flexibilidade).


This study evaluated and compared the bending resistance of rotary endodontic instruments made of conventional nickel-titanium (NiTi) and M-wire by means of cantilever bending test. The flexibility of an endodontic instrument depends on its chemical composition and the thermo mechanical treatment of the alloy, as well as on its cross-sectional geometry on the helical shaft of the endodontic instrument. The results showed that the Profile Vortex instruments, made from NiTi wires called M-wire, had the greatest bending resistance (lowest flexibility), while RaCe instruments, produced from conventional NiTi wires showed the lowest bending resistance (greatest flexibility) among the instruments tested.


Assuntos
Tratamento do Canal Radicular/instrumentação , Resistência à Flexão
19.
ROBRAC ; 19(48)abr. 2010. tab
Artigo em Português | LILACS | ID: lil-558310

RESUMO

No presente trabalho avaliou-se e comparou-se a carga necessária para induzir uma determinada deformação elástica de instrumentos endodônticos de NiTi mecanizados de mesmo número e de quatro marcas comerciais. Nos ensaios mecânicos de flexão em cantilever os instrumentos foram fixados em uma das extremidades e a carga aplicada na extremidade oposta. Os resultados obtidos demonstraram que em termos de flexibilidade: TF > BioRace > K3 > ProTaper.


In the present study evaluated and compared the load required to induce a certain elastic deformation of NiTi endodontic instruments mechanized same number and four trademarks. In the mechanical cantilever bending the instruments were set at one end and the load applied at the opposite end. The results showed that in terms of flexibility: TF> BioRace> K3> ProTaper.

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