Powders of Diamond Nanoparticles as a Promising Material for Reflectors of Very Cold and Cold Neutrons.

More than 15 years ago, the study of nanodiamond (ND) powders as a material for designing reflectors of very cold neutrons (VCNs) and cold neutrons (CNs) began. Such reflectors can significantly increase the efficiency of using such neutrons and expand the scope of their application for solving applied and fundamental problems. This review considers the principle of operation of VCN and CN reflectors based on ND powders and their advantages. Information is presented on the performed experimental and theoretical studies of the effect of the size, structure, and composition of NDs on the efficiency of reflectors. Methods of chemical and mechanical treatments of powders in order to modify their chemical composition and structure are discussed. The aim is to avoid, or at least to decrease, the neutron inelastic scatterers and absorbers (mainly hydrogen atoms but also metallic impurities and nitrogen) as well as to enhance coherent elastic scattering (to destroy ND clusters and sp2 carbon shells on the ND surface that result from the preparation of NDs). Issues requiring further study are identified. They include deeper purification of NDs from impurities that can be activated in high radiation fluxes, the stability of NDs in high radiation fluxes, and upscaling methods for producing larger quantities of ND powders. Possible ways of solving these problems are proposed.

New Material Exploration to Enhance Neutron Intensity below Cold Neutrons: Nanosized Graphene Flower Aggregation.

It is proposed that nanosized graphene aggregation could facilitate coherent neutron scattering under particle size conditions similar to nanodiamonds to enhance neutron intensity below cold neutrons. Using the RIKEN accelerator-driven compact neutron source and iMATERIA at J-PARC, we performed neutron measurement experiments, total neutron cross-section and small-angle neutron scattering on nanosized graphene aggregation. For the first time, the measured data revealed that nanosized graphene aggregation increased the total neutron cross-sections and small-angle scattering in the cold neutron energy region. This is most likely due to coherent scattering, resulting in higher neutron intensities, similar to nanodiamonds.

External water transport is more important than vascular transport in the extreme atmospheric epiphyte Tillandsia usneoides (Spanish moss).

Most epiphytic bromeliads, especially those in the genus Tillandsia, lack functional roots and rely on the absorption of water and nutrients by large, multicellular trichomes on the epidermal surfaces of leaves and stems. Another important function of these structures is the spread of water over the epidermal surface by capillary action between trichome "wings" and epidermal surface. Although critical for the ultimate absorption by these plants, understanding of this function of trichomes is primarily based on light microscope observations. To better understand this phenomenon, the distribution of water was followed by its attenuation of cold neutrons following application of H2 O to the cut end of Tillandsia usneoides shoots. Experiments confirmed the spread of added water on the external surfaces of this "atmospheric" epiphyte. In a morphologically and physiologically similar plant lacking epidermal trichomes, water added to the cut end of a shoot clearly moved via its internal xylem and not on its epidermis. Thus, in T. usneoides, water moves primarily by capillarity among the overlapping trichomes forming a dense indumentum on shoot surfaces, while internal vascular water movement is less likely. T. usneoides, occupying xeric microhabitats, benefits from reduction of water losses by low-shoot xylem hydraulic conductivities.

Prompt Gamma-ray Activation Analysis for Certification of Sulfur in Fuel Oil SRMs.

A combination of cold neutron prompt gamma-ray activation analysis (CNPGAA) and thermal neutron (TN) PGAA was used to determine sulfur in fuel oils to develop a method to provide values for certification. CNPGAA was used to measure S/H mass ratios, and TNPGAA to measure hydrogen mass fractions. Measurements were combined to determine sulfur mass fractions (with expanded uncertainties) of 2.159 % ± 0.072 % for SRM 1622e, 0.7066 % ± 0.0120 % for SRM 1619b, and 0.1266 % ± 0.0030 % for SRM 1617b, in agreement with certified values. The results validate the method as suitable for certification of sulfur at mass fractions ≥ 0.1 %.

The Fundamental Neutron Physics Facilities at NIST.

The program in fundamental neutron physics at the National Institute of Standards and Technology (NIST) began nearly two decades ago. The Neutron Interactions and Dosimetry Group currently maintains four neutron beam lines dedicated to studies of fundamental neutron interactions. The neutrons are provided by the NIST Center for Neutron Research, a national user facility for studies that include condensed matter physics, materials science, nuclear chemistry, and biological science. The beam lines for fundamental physics experiments include a high-intensity polychromatic beam, a 0.496 nm monochromatic beam, a 0.89 nm monochromatic beam, and a neutron interferometer and optics facility. This paper discusses some of the parameters of the beam lines along with brief presentations of some of the experiments performed at the facilities.

LENS: A New Pulsed Neutron Source for Research and Education.

A new pulsed neutron source is under construction at the Indiana University Cyclotron Facility (IUCF). Neutrons are produced via (p,n) reactions by a low-energy proton beam incident on a thin beryllium target. The source is tightly coupled to a cold methane moderator held at a temperature of 20 K or below. The resulting time-averaged cold neutron flux is expected to be comparable to that of the Intense Pulsed Neutron Source (IPNS) facility at Argonne National Laboratory. The initial experimental suite will include instrumentation for small angle neutron scattering (SANS), moderator studies, radiography, and zero-field spin-echo SANS.

Parity-Violating Neutron Spin Rotation in a Liquid Parahydrogen Target.

Our understanding of hadronic parity violation is far from clear despite nearly 50 years of theoretical and experimental progress. Measurements of low-energy parity-violating observables in nuclear systems are the only accessible means to study the flavor-conserving weak hadronic interaction. To reduce the uncertainties from nuclear effects, experiments in the few and two-body system are essential. The parity-violating rotation of the transverse neutron polarization vector about the momentum axis as the neutrons traverse a target material has been measured in heavy nuclei and few nucleon systems using reactor cold neutron sources. We describe here an experiment to measure the neutron spin-rotation in a parahydrogen target (n-p system) using pulsed cold-neutrons from the fundamental symmetries beam line at the Spallation Neutron Source under construction at the Oak Ridge National Laboratory.

Measurement of the Parity-Violating Neutron Spin Rotation in (4) He.

In the meson exchange model of weak nucleon-nucleon (NN) interactions, the exchange of virtual mesons between the nucleons is parameterized by a set of weak meson exchange amplitudes. The strengths of these amplitudes from theoretical calculations are not well known, and experimental measurements of parity-violating (PV) observables in different nuclear systems have not constrained their values. Transversely polarized cold neutrons traveling through liquid helium experience a PV spin rotation due to the weak interaction with an angle proportional to a linear combination of these weak meson exchange amplitudes. A measurement of the PV neutron spin rotation in helium (φ PV ( n ,α)) would provide information about the relative strengths of the weak meson exchange amplitudes, and with the longitudinal analyzing power measurement in the p + α system, allow the first comparison between isospin mirror systems in weak NN interaction. An earlier experiment performed at NIST obtained a result consistent with zero: φ PV ( n ,α) = (8.0 ±14(stat) ±2.2(syst)) ×10(-7) rad / m[1]. We describe a modified apparatus using a superfluid helium target to increase statistics and reduce systematic effects in an effort to reach a sensitivity goal of 10(-7) rad/m.

Observation on the Visibility Decrease in a VCN Spin Resonator Interferometry.

The present paper reports on the detailed studies concerning the neutron spin interference visibility observed after transmitting through multilayer magnetic resonators in a spin echo condition with very cold neutrons from a high flux reactor. The observed visibility of the interference between upward and downward spin components perpendicular to the Larmor precession plane of the neutron spin are compared with the numerical simulations in the plane wave theory and also in the Schrödinger wave-packet model. The comparison revealed the instructive characteristic features of obvious additional visibility decrease observed in the interference between the tunnelling and refractive transmissions of each spin components in a single as well as a couple of multilayer magnetic resonators.

On the Measurement of the Neutron Lifetime Using Ultracold Neutrons in a Vacuum Quadrupole Trap.

We present a conceptual design for an experiment to measure the neutron lifetime (~886 s) with an accuracy of 10(-4). The lifetime will be measured by observing the decay rate of a sample of ultracold neutrons (UCN) confined in vacuum in a magnetic trap. The UCN collaboration at Los Alamos National Laboratory has developed a prototype UCN source that is expected to produce a bottled UCN density of more than 100/cm(3) [1]. The availability of such an intense source makes it possible to approach the measurement of the neutron lifetime in a new way. We argue below that it is possible to measure the neutron lifetime to 10(-4) in a vacuum magnetic trap. The measurement involves no new technology beyond the expected UCN density. If even higher densities are available, the experiment can be made better and/or less expensive. We present the design and methodology for the measurement. The slow loss of neutrons that have stable orbits, but are not energetically trapped would produce a systematic uncertainty in the measurement. We discuss a new approach, chaotic cleaning, to the elimination of quasi-neutrons from the trap by breaking the rotational symmetry of the quadrupole trap. The neutron orbits take on a chaotic character and mode mixing causes the neutrons on the quasi-bound orbits to leave the trap.

Project of Neutron Beta-Decay A-Asymmetry Measurement With Relative Accuracy of (1-2)×10(-3).

We are going to use a polarized cold neutron beam and an axial magnetic field in the shape of a bottle formed by a superconducting magnetic system. Such a configuration of magnetic fields allows us to extract the decay electrons inside a well-defined solid angle with high accuracy. An electrostatic cylinder with a potential of 25 kV defines the detected region of neutron decays. The protons, which come from this region will be accelerated and registered by a proton detector. The use of coincidences between electron and proton signals will allow us to considerably suppress the background. The final accuracy of the A-asymmetry will be determined by the uncertainty of the neutron beam polarization measurement which is at the level of (1-2) × 10(-3), as shown in previous studies.

Search for Radiative ß-Decay of the Free Neutron.

Results of the first experiment to search for the radiative decay mode of the free neutron are reported. The γ-spectrum was studied in the energy region from 35 keV to 100 keV in six Cs(Tl) scintillators, each set at an angle of 35° to, and shielded from, a central plastic scintillator electron detector. Triple coincidences were recorded with recoil protons detected in a micro-channel plate. A limit for the branching ratio BR < 6.9 × 10(-3) (90 % confidence level) was obtained, which is greater that the theoretical prediction by not more than a few tenths of a percent.

Development of a Position Sensitive Neutron Detector with High Efficiency and Energy Resolution for Use at High-Flux Beam Sources.

We are developing a high-efficiency neutron detector with 1 cm position resolution and coarse energy resolution for use at high-flux neutron source facilities currently proposed or under construction. The detector concept integrates a segmented (3)He ionization chamber with the position sensitive, charged particle collection methods of a MicroMegas detector. Neutron absorption on the helium produces protons and tritons that ionize the fill gas. The charge is amplified in the field region around a wire mesh and subsequently detected in current mode by wire strips mounted on a substrate. One module consisting of a high-voltage plate, a field-shaping high-voltage plate, a grid and wire strips defines a detection region. For 100 % efficiency, detector modules are consecutively placed along the beam axis. Analysis over several regions with alternating wire strip orientation provides a two-dimensional beam profile. By using (3)He, a 1/v absorption gas, each axial region captures neutrons of a different energy range, providing an energy-sensitive detection scheme especially useful at continuous beam sources.

The NIST Cold Neutron Research Facility.

The Cold Neutron Research Facility (CNRF) at the National Institute of Standards and Technology (NIST) Research Reactor (NBSR) is now coming on line, with the first seven experimental stations operational, and more stations scheduled to be installed during 1992. The present article provides an introduction to the facility, and to other articles in the current issue that give more details on some of the research opportunities that the facility will bring to NIST.

Neutron Depth Profiling: Overview and Description of NIST Facilities.

The Cold Neutron Depth Profiling (CNDP) instrument at the NIST Cold Neutron Research Facility (CNRF) is now operational. The neutron beam originates from a 16 L D2O ice cold source and passes through a filter of 135 mm of single crystal sapphire. The neutron energy spectrum may be described by a 65 K Maxwellian distribution. The sample chamber configuration allows for remote controlled scanning of 150 × 150 mm sample areas including the varying of both sample and detector angle. The improved sensitivity over the current thermal depth profiling instrument has permitted the first nondestructive measurements of 17O profiles. This paper describes the CNDP instrument, illustrates the neutron depth profiling (NDP) technique with examples, and gives a separate bibliography of NDP publications.