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1.
J Esthet Restor Dent ; 36(10): 1466-1476, 2024 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-39082969

RESUMO

OBJECTIVE: This study evaluated the completeness and accuracy of information in LCU instruction manuals from 40 manufacturers. MATERIALS AND METHODS: Instruction manuals from 40 LCUs (20 from leading manufacturers and 20 budget units) were reviewed. Twenty-eight parameters across five categories were assessed using a binary scale (0=incorrect/missing, 1=correct). The categories and their respective evaluation scores were: LCU characteristics (43%), instructions for use (7%), safety precautions (14%), maintenance recommendations (29%), and regulatory certification (7%). These scores were combined to produce a final score. RESULTS: Scores from leading manufacturers ranged between 46-86%, while the budget category ranged from 18-68%. All manuals provided information about the wavelength/spectrum of the LCU. Only Valo X and Valo Cordless reported power values and used the term "irradiance" instead of "intensity." Details such as LED type and active tip emission area were often missing. Instructions on how to use the LCU to photo-cure resins were frequently limited. Although most manuals addressed safety precautions, several lacked details on heat issues and general health precautions. All manuals included maintenance instructions, though information on replacement parts was often missing. Among the LCUs, 85% stated they were CE certified, 32% held both FDA and CE certification, and 63% claimed compliance with ISO and/or IEC standards. CONCLUSIONS: There were notable differences in the completeness and accuracy of the instruction manuals. Manuals from major manufacturers generally provided more comprehensive information than their budget counterparts. CLINICAL SIGNIFICANCE: Instruction manuals should contain accurate information to help clinicians deliver the highest standard of care. The lack of important information about the LCUs in the manuals is concerning.


Assuntos
Lâmpadas de Polimerização Dentária , Humanos , Manuais como Assunto
2.
Clin Cosmet Investig Dent ; 16: 153-165, 2024.
Artigo em Inglês | MEDLINE | ID: mdl-38808075

RESUMO

Aim: This study aimed to evaluate the effects of polywave and monowave light-emitting diode curing units on the microtensile bond strength and failure types of three bulk-fill resin composites. Materials and Methods: This in vitro experimental study was performed on 180 microbars obtained from human third molars and were distributed into 12 groups according to the type of bulk-fill resin composite and the light-curing unit. Third molars were restored using Filtek One Bulk Fill Restorative, Tetric® N-Ceram Bulk Fill, and Opus Bulk Fill resin composites was light-cured with Elipar Deep Cure L and Valo in three modes: standard, high power, and extra power. Subsequently, microtensile analysis was carried out with a universal testing machine and the type of failure with an optical stereomicroscope. For statistical analysis, the Kruskal-Wallis H-test was used, with the Bonferroni post hoc test and Fisher's exact test, considering a significance of p<0.05. Results: There were significant differences in the microtensile bond strength between the Filtek One Bulk Fill restorative and Opus Bulk-Fill (p = 0.042) when light was cured with the polywave unit at standard power. On the other hand, the Filtek One Bulk Fill Restorative and Opus Bulk Fill resins showed significant differences in microtensile bond strength when light was cured with the monowave unit compared with the polywave unit (p<0.05). Conclusion: The presence of alternative photoinitiator systems that are more reactive than camphorquinone produced higher microtensile bond strength in Tetric N-Ceram Bulk Fill and Opus Bulk Fill resins when light-cured with a high and standard polywave unit, respectively, compared to Filtek One Bulk Fill resins. Finally, Tetric N-Ceram Bulk Fill and Opus Bulk Fill resins had the highest percentage of mixed failures, while Filtek One Bulk Fill resin had adhesive failures, which was related to its lower microtensile bond strength.

3.
Acta Stomatol Croat ; 58(1): 30-38, 2024 Mar.
Artigo em Inglês | MEDLINE | ID: mdl-38562217

RESUMO

Objective: The aim of this study was to compare the light transmission of monowave and polywave-curing devices by a bulk-fill composite containing only camphorquinone as a photoinitiator. Materials and methods: Three light-curing devices were used to cure bulk-fill composite QuiXfil: one monowave (Translux® Wave) and two polywave (VALO Cordless and Bluephase® PowerCure. The NIST-calibrated spectrometer (MARC Resin Calibrator, BlueLight Analytics Inc.) was used to measure the incident and transmitted light through a 2-mm composite specimen over 20 s. Light transmittance was calculated from the ratio of the amount of transmitted and incident light. For data analysis (ANOVA, α = 0.05), total irradiation of the entire spectrum, irradiation with wavelengths of 360-420 nm for the violet spectrum, and 420-540 nm for the blue spectrum were selected. Results: Monowave curing unit Translux® Wave had the lowest light transmission (13.78 ± 0.5%), similar to the violet light transmission of polywave devices (12.02 ± 0.94% and 13.81 ± 1.72% for Valo Cordless and Bluephase PowerCure, respectively). Blue light transmittance (32.15-23.70%) was more than twofold higher than for the wavelengths in the violet region of the spectrum (13.81-12.02%) for the two polywave devices. VALO Cordless showed the highest total and blue light transmission (p<0.001). There was no significant difference in the transmission of the violet part of the spectrum between VALO Cordless and Bluephase® PowerCure (p = 0.465). Conclusion: Within the limitations of this study, we could conclude that polywave curing devices can be used for the polymerization of the bulk-fill composite with camphorquinone as the sole photoinitiator.

4.
Bioinformation ; 19(13): 1353-1358, 2023.
Artigo em Inglês | MEDLINE | ID: mdl-38415033

RESUMO

The effect of altering the distance between light tip and outer layer of composite (DLR) on the depth of composite cure with a range of low to high light intensity curing lamps and with different types of light unit is of interest. Three LED units (T= Freelight,U = Ultrablue IS, V = Coltolux LED, one PAC unit (S=PAC) and three halogen light-curing units (P = XL2500, Q = HelioluxVL, R = Visiolux) were analyzed. A human molar tooth that was separated mesio-distally to buccal and lingual halves was used to create a natural tooth sample. Data shows that the depth of cure for the composite material decreased as the distance between the repair and the light source increased. There was no appreciable difference in performance between the LEDs and the other kinds of curing lamps as the distance between them grew.

5.
Dent Clin North Am ; 66(4): 537-550, 2022 10.
Artigo em Inglês | MEDLINE | ID: mdl-36216445

RESUMO

This article focuses on the current understanding and concerns over the blue-light hazard when using dental light-curing units. It also provides information and safety protocols to guide the practitioner in making important decisions regarding dental personnel's health and the quality of dental restorations.


Assuntos
Lâmpadas de Polimerização Dentária , Cura Luminosa de Adesivos Dentários , Resinas Compostas , Humanos
6.
Saudi Dent J ; 34(5): 362-368, 2022 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-35814845

RESUMO

Objectives: To evaluate the effect of light curing unit (LCU) types and distance from light curing unit tip on the translucency parameters (TP) of bulk fill composite materials. Materials and Methods: Two bulk-fill resin composites and one nanohybrid composite were used in this study. The specimens were divided into groups based on the type of curing unit used, and further subdivided based on the distance of the curing source to the surface of the resin composite. Translucency was evaluated at 4 mm thickness (for the bulk-fill) and 2 mm thickness (for nanohybrid) after curing using two different light curing units at zero, 2 mm, and 4 mm distance. The results were analyzed using two-way ANOVA at the significance level of a p-value of < 0.05. Results: Among all the tested materials, Filtek Bulk Fill Posterior RBC showed the highest TP at 0 mm distance when cured with Blue phase G2 LED LCU and it was the least affected by the differences in distances. However, Filtek Z350 nanohybrid composite had no significant differences between the three distances when cured with Blue phase G2 LCU. Conclusion: Translucency values among the studied bulk-fill materials are affected by material composition, curing units and the distance of the tip of the light source to the restoration surface.

7.
J Dent ; 122: 104141, 2022 07.
Artigo em Inglês | MEDLINE | ID: mdl-35483497

RESUMO

OBJECTIVES: To evaluate the depth of cure (DOC) of ten contemporary resin-based composites (RBCs), light-cured using different LCUs and exposure times. METHODS: The power, radiant emittance, irradiance, radiant exposure (RE), and beam profiles from a laser (M, Monet), a multi-peak (V, Valo Grand), and single-peak (S, SmartLite Pro) LCU were measured. The DOC was measured using a 6-mm diameter metal mold and a solvent dissolution method to remove the uncured RBC. The length of the remaining RBC was divided by 2. The exposure times were: 1 s and 3 s for M, 10 s and 20 s for V, and 10 s and 20 s for S. Data were analyzed using: Bland-Altman distribution, Pearson's Correlation, and an artificial neural network (ANN) to establish the relative importance of the factors on the DOC (α=0.05; ß=0.2). RESULTS: Significant differences were found in the DOC achieved by the different LCUs and composites. The laser LCU emitted the highest power, radiant emittance is used above and in the tables and delivered the highest irradiance. However, this LCU used for 1 s delivered the lowest RE and produced the shortest DOC in all ten RBCs. The ANN demonstrated that the RE is the most critical factor for the DOC. Bland-Altman comparisons showed that the DOCs achieved with the laser LCU used for 1 s were between 17 and 34% shorter than the other conditions. CONCLUSIONS: Although the laser LCU cured all 10 RBCs when used for 1 s, it produced the shallowest DOC, and some RBCs did not achieve their minimum DOC threshold. The RE and not the irradiance was the most important factor in determining the DOC of these 10 RBCs. CLINICAL SIGNIFICANCE: Despite delivering high power and irradiance, the laser used for l s delivered a lower radiant exposure than the conventional LCUs used for 10 s. This resulted in a shorter DOC.


Assuntos
Resinas Compostas , Lâmpadas de Polimerização Dentária , Materiais Dentários , Lasers , Teste de Materiais , Polimerização
8.
J Contemp Dent Pract ; 23(8): 775-780, 2022 Aug 01.
Artigo em Inglês | MEDLINE | ID: mdl-37283010

RESUMO

AIM: The aim was to find out whether the light-tip distance affected the shear bond strength of orthodontic brackets when cured with light-emitting diode (LED) and high-intensity LED at four different light-tip distances. MATERIALS AND METHODS: Extracted human premolars were divided into eight groups. Each tooth was embedded in the self-cure acrylic resin block, and brackets were bonded and cured with different lights and different distances. Shear bond strength tests were performed in vitro using the universal testing machine. Data were analyzed using one-way ANOVA test. RESULTS: The descriptive statistics for shear bond strength of orthodontic brackets cured with LED light at 0 mm was 8.49 ± 1.08 MPa, at 3 mm was 8.13 ± 0.85 MPa, 6 mm was 6.42 ± 0.42 MPa, and at 9 mm was 5.24 ± 0.92 MPa, and those cured with high-intensity light at 0 mm was 19.23 ± 4.83 MPa, at 3 mm was 17.65 ± 3.28 MPa, at 6 mm was 13.04 ± 2.36 MPa, and at 9 mm was 11.74 ± 1.4 MPa. Mean shear bond strength was found to decrease as the light-tip distance increased with both light sources. CONCLUSION: Shear bond strength is higher when the light source is close to the surface to be cured, and it decreases as the distance increases. The highest shear bond strength was achieved with high-intensity light. CLINICAL SIGNIFICANCE: Light-emitting diode or high-intensity units can be used for bonding orthodontic brackets without compromising the shear bond strength of the brackets, and that shear bond strength is stronger when the light source is close to the surface to be cured, and it decreases as the distance increases between the light source and the surface.


Assuntos
Colagem Dentária , Braquetes Ortodônticos , Humanos , Análise do Estresse Dentário , Teste de Materiais , Dente Pré-Molar , Resistência ao Cisalhamento , Estresse Mecânico , Cimentos de Resina/química , Propriedades de Superfície
9.
Materials (Basel) ; 14(22)2021 Nov 13.
Artigo em Inglês | MEDLINE | ID: mdl-34832251

RESUMO

The aim of this study was to compare three different light-curing-units (LCUs) and determine their effectiveness in the adhesive cementation of indirect composite restorations when a light-curing resin cement is used. Two resin composites were selected: Enamel Plus HRI (Micerium) and AURA (SDI). Three thicknesses (3 mm, 4 mm and 5 mm) were produced and applied as overlays and underlays for each resin composite. A standardized composite layer was placed between underlay and overlay surfaces. Light curing of the resin-based luting composites was attained through the overlay filters using LCUs for different exposure times. All specimens were allocated to experimental groups according to the overlay thickness, curing unit and curing time. Vickers Hardness (VH) notches were carried out on each specimen. Data were statistically evaluated. The curing unit, curing time and overlay thickness were significant factors capable of influencing VH values. The results showed significantly decreased VH values with increasing specimen thickness (p < 0.05). Significant differences in VH values were found amongst the LCUs for the various exposure times (p < 0.05). According to the results, a time of cure shorter than 80 s (with a conventional quartz-tungsten-halogen LCU) or shorter than 40 s (with a high-power light-emitting diode (LED) LCU) is not recommended. The only subgroup achieving clinically acceptable VH values after a short 20 s curing time included the 3 mm-thick overlays made out of the AURA composite, when the high-power LED LCU unit was used (VH 51.0). Composite thickness has an intense effect on polymerization. In clinical practice, light-cured resin cements may result in insufficient polymerization for high thickness and inadequate times. High-intensity curing lights can attain the sufficient polymerization of resin cements through overlays in a significantly shorter time than conventional halogen light.

10.
Odontology ; 109(4): 874-883, 2021 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-34023954

RESUMO

To determine the influence of light curing units (LCUs) and material viscosity on the degree of conversion (DC) of bulk-fill (BF) resin-based composites (RBCs) placed in deep cavity preparations. Four LCUs were tested: Valo cordless, Bluephase-G2, Poly wireless and Radii-cal. Light irradiance was determined at 0 mm and 6 mm distance to the reading sensor. The following RBCs were considered: Filtek BF, Filtek BF Flow, Opus BF, Opus BF Flow, Tetric N-Ceram BF and Surefil SDR Flow. Sirius-Z was used with the incremental technique. DC (n = 3) was evaluated by spectroscopy both at top and bottom regions of deep preparations with 6 mm depth. The data were submitted to ANOVA and Tukey's test (α = 0.05). Pearson's correlation (95%) was used to verify the relation between the LCUs and the curing potential of RBCs. The DC at 6 mm depth was reduced when Opus BF, Opus BF Flow and Tetric N-Ceram BF were activated with Radii-cal. There was a positive correlation between the LCU irradiance and the bottom/top conversion ratios. The materials' viscosities did not affect the curing potential. Bulk-fill composites did not present higher curing potential than the conventional composite used with the incremental technique; the most important aspect of the LCU was the irradiance ratio; and the materials' viscosity did not affect the curing potential as a function of depth. Radii-cal negatively impacted the degree of conversion at 6 mm depth for most bulk-fill resin composites. Depending on the brand, bulk-fill composites may present reduced curing potential due to the light source when placed in deep cavities. Dentists should avoid LCU with acrylic tips to photoactivate bulk-fill resin-based composites.


Assuntos
Lâmpadas de Polimerização Dentária , Teste de Materiais , Polimerização , Propriedades de Superfície , Viscosidade
11.
Odovtos (En línea) ; 23(1)abr. 2021.
Artigo em Inglês | LILACS, SaludCR | ID: biblio-1386506

RESUMO

Abstract: The aim of this study was to evaluate and compare the effects of different light sources on shear bond strength when bulk-fill composite was used for the repair of different composite resins. A total of 126 samples made from six resin composites with different properties were aged (thermal-cycling with 5000 cycle), exposed to the same surface treatments and adhesive procedure. Then, they were repaired with a bulk-fill composite. At the polymerization step, each group was divided into three subgroups (n=7) and light cured with a QTH light source for 40s and two different LED light sources for 20s. Subsequently, the specimens were aged in distilled water at 37 ºC for 4 weeks and then subjected to shear bond strength test. Then, the specimens were examined under a stereomicroscope to identify modes of failure and visualized by Scanning Electron Microscope. Data obtained from the study were analyzed using ANOVA and Tukey HSD Test (α=0.05). In all groups, the light curing units had an impact on shear bond strength (p<0.05). Among the study groups, the greatest bond strength values were observed in the specimens repaired using the LED and the specimens repaired with the QTH light curing unit had the lowest bond strength values. It was concluded that the content of composite resins and light curing units may influence bond strength of different composites repaired with the bulk-fill composite.


Resumen: El objetivo de este estudio fue evaluar y comparar los efectos de diferentes fuentes de luz sobre la resistencia de la unión al cizallamiento cuando se utiliza una resina bulk-fill para la reparación de diferentes resinas compuestas. Se envejecieron un total de 126 muestras fabricadas con seis compuestos de resina con diferentes propiedades (ciclo térmico con 5000 ciclos), expuestas a los mismos tratamientos de superficie y procedimiento adhesivo. Luego, fueron reparadas con una resina bulk- fill. En el paso de polimerización, cada grupo fue dividido en tres subgrupos (n=7) y fotopolimerizado con una fuente de luz QTH por 40s y dos fuentes de luz LED por 20s. Posteriormente, los especímenes se envejecieron en agua destilada a 37 ºC durante 4 semanas y luego se sometieron a una prueba de resistencia adhesiva de cizalla. Luego, los especímenes fueron examinados bajo un estereomicroscopio para identificar los modos de falla y visualizados por el Microscopio Electrónico de Barrido. Los datos obtenidos del estudio fueron analizados usando el ANOVA y la prueba Tukey HSD (α=0.05). En todos los grupos, las unidades de fotopolimerización tuvieron un impacto en la fuerza de adhesión al cizallamiento (p<0,05). Entre los grupos de estudio, los mayores valores de fuerza de adhesión se observaron en los especímenes reparados utilizando el LED y los especímenes reparados con la unidad de fotopolimerización QTH tuvieron los valores de fuerza de adhesión más bajos. Se llegó a la conclusión de que el contenido de las resinas compuestas y las unidades de fotopolimerización pueden influir en la fuerza de adhesión de los diferentes compuestos reparados con resinas bulk-fill.


Assuntos
Cura Luminosa de Adesivos Dentários/métodos , Reparação de Restauração Dentária
13.
J Dent ; 105: 103568, 2021 02.
Artigo em Inglês | MEDLINE | ID: mdl-33385531

RESUMO

OBJECTIVE: This study correlates the mechanical and biological response of commercially available resin-based composites (RBCs) to clinically relevant light-curing conditions. METHODS: Two RBCs (Venus and Venus Pearl; Kulzer) that use different monomer and photo-initiator systems, but have a similar filler volume and shade, were exposed to either just blue light, or violet and blue light from two different LCUs (Translux Wave and Translux 2Wave; Kulzer). Distance and exposure times were adjusted so that both LCUs delivered 5 similar levels of radiant exposures (RE) between 1.5 J/cm²-25 J/cm² in the blue wavelength range. Thus, the violet light was additional light. The top and bottom of 2-mm thick specimens were subjected to a depth-sensing indentation test (Martens hardness/HM, Vickers hardness/HV, indentation modulus/YHU, mechanical work/Wtotal, plastic deformation work/Wplas, creep/Cr). The viability of human gingival fibroblasts was assessed after three days of exposure to RBC eluates. One and multiple-way analysis of variance (ANOVA), the Tukey honestly significant difference (HSD) post-hoc tests (α = 0.05), t-test and a Spearman correlation analysis were used. RESULTS: As the RE increased, the mechanical properties increased at a greater rate at the top compared to the bottom of the RBCs. Values measured at the bottom of 2-mm increments approached the values measured at the top only when RE > 25 J/cm² of blue light was delivered. Toxicity decreased with RE and elution cycles and was lower for Venus Pearl. Within one RE level, addition of violet light resulted in significantly improved properties (in 131 out of 150 comparisons, p < 0.05). This effect was stronger for Venus Pearl. There was a good correlation between mechanical and biological parameters. This correlation decreased as the number of eluates increased. CLINICAL SIGNIFICANCE: The mechanical and biological response to variation in RE is interrelated. The addition of violet light has a positive effect, particularly at low RE.


Assuntos
Resinas Compostas , Lâmpadas de Polimerização Dentária , Materiais Dentários , Dureza , Humanos , Cura Luminosa de Adesivos Dentários , Teste de Materiais , Polimerização , Propriedades de Superfície
14.
Dent Mater J ; 40(1): 44-51, 2021 Jan 31.
Artigo em Inglês | MEDLINE | ID: mdl-32848103

RESUMO

This study aimed to assess the influence of different light curing units (LCUs) on the polymerization of various flowable resin composites. Three LCUs (Optilux 501, Elipar™ DeepCure-L LED and Bluephase®20i) and eight flowable resin composites: MI FIL Flow, Estelite Flow Quick, Estelite Universal Flow (medium), Estelite Universal Flow (super low), Beautifil Flow Plus, Clearfil Majesty ES Flow, Filtek Supreme Ultra flowable and TetricEvo Flow were tested. For Vickers microhardness (VHN) test and degree of conversion (DC), specimens were prepared and polymerized for 20 s. VHN test was performed at top surfaces (3 indentations) and DC for each specimen was measured using Fourier transform infrared (FT-IR) spectroscopy after 24 h dry storage in dark at 37˚C. The data were analyzed with 2-way ANOVA and t-test with Bonferroni correction. DC and hardness values showed a relationship between materials and LCUs. The curing efficacy of LCU type may depend on the material composition.


Assuntos
Lâmpadas de Polimerização Dentária , Cura Luminosa de Adesivos Dentários , Resinas Compostas , Dureza , Teste de Materiais , Polimerização , Espectroscopia de Infravermelho com Transformada de Fourier , Propriedades de Superfície
15.
Dent Mater J ; 39(6): 976-983, 2020 Dec 03.
Artigo em Inglês | MEDLINE | ID: mdl-32727961

RESUMO

This study investigated the effect of high-irradiance light-curing on exposure time and pulpal temperature of adequately-cured composite. Composite placed in a molar preparation was cured using high-irradiance light-curing units (Flashmax P3, Valo, S.P.E.C. 3 LED, Cybird XD) and tested for hardness occlusal-gingivally. The first group had exposure times set according to manufacturer settings (recommended), second group to yield 80% of maximum hardness at the 2 mm depth (experimental), and third group was set at 20 s (extended). Exposure time necessary to adequately polymerize the composite at 2 mm depth was 9 s for the Cybird XD and Valo and 12 s for S.P.E.C. 3 LED and Flashmax P3. None of the high-irradiance light-curing units adequately polymerized the composite at the manufacturer-recommended minimum-exposure times of 1-3 s. Exposure times necessary to adequately polymerize composite at 2 mm resulted in a maximum pulpal-temperature increase well below the temperature associated with possible pulpal necrosis.


Assuntos
Resinas Compostas , Lâmpadas de Polimerização Dentária , Dureza , Cura Luminosa de Adesivos Dentários , Teste de Materiais , Temperatura , Tempo
16.
J Oral Sci ; 62(3): 288-292, 2020 Jun 23.
Artigo em Inglês | MEDLINE | ID: mdl-32475863

RESUMO

The purpose of this study was to determine the depth of cure and the type and amount of monomers released from bulk-fill composites in different curing protocols. Five different composite resins Filtek Bulk-Fill Posterior, Filtek Bulk-Fill Flowable, SureFil SDR, X-tra Fil, and X-tra base, were used. A light-emitting diode (LED) device was used in 3 different modes (standard, high power, and extra power mode), and a halogen light device was also used as a control. Surface hardness was measured and the depth of cure was calculated. Monomer analysis was performed using high performance liquid chromatography (HPLC). The data were analyzed using Tamhane's T2 post-hoc test (α = 0.05). The cure depth for all materials except for Filtek Bulk-Fill Posterior (extra power mode) and Filtek Bulk-Fill Flowable (high power and extra power modes) was over 80%. Under the conditions of this study, the amount of monomer released from composite resins changed according to the type of composite resin and the light mode used.


Assuntos
Resinas Compostas , Materiais Dentários , Dureza , Teste de Materiais , Polimerização , Propriedades de Superfície
17.
Adv Clin Exp Med ; 27(4): 469-476, 2018 Apr.
Artigo em Inglês | MEDLINE | ID: mdl-29558043

RESUMO

BACKGROUND: More than 35 substances released from composite fillings have been identified. Among these, basic monomers and the so-called co-monomers are most often reported. The substances released from polymer-based materials demonstrate allergenic, cytotoxic, genotoxic, mutagenic, embryotoxic, teratogenic, and estrogenic properties. OBJECTIVES: The aim of this study was to measure the amounts of triethylene glycol dimethacrylate (TEGDMA) and urethane dimethacrylate (UDMA) monomers released from composite dental fillings to citrate-phosphate buffer with the pH of 4, 6, 8 after 24 h and 6 months from the polymerization. MATERIAL AND METHODS: Ten samples for each polymerization method had been made from the composite material (Filtek Supreme XT, 3M ESPE, St. Paul, USA), which underwent polymerization using the following lamps: halogen lamp (Translux CL, Heraeus Kulzer, Hanau, Germany) (sample H) and diode lamp (Elipar Freelight 2, 3M ESPE), with soft start function (group DS) and without that function (group DWS). RESULTS: It has been demonstrated that the type of light-curing units has a significant impact on the amount of TEGDMA and UDMA released. The amount of UDMA and TEGDMA monomers released from composite fillings differed significantly depending on the source of polymerization applied, as well as the pH of the solution and sample storage time. CONCLUSIONS: Elution of the monomers from composite material polymerized using halogen lamp was significantly greater as compared to curing with diode lamps.


Assuntos
Resinas Compostas/química , Materiais Dentários , Metacrilatos/química , Polietilenoglicóis , Ácidos Polimetacrílicos , Poliuretanos , Bis-Fenol A-Glicidil Metacrilato , Halogênios , Humanos , Teste de Materiais , Polimerização
18.
Materials (Basel) ; 10(1)2017 Jan 14.
Artigo em Inglês | MEDLINE | ID: mdl-28772427

RESUMO

This study investigated the impact of different light curing units (LCUs) for the polymerization of adhesive system visio.link (VL) on the tensile bond strength (TBS) of different PEEK compositions. For TBS measurements, 216 PEEK specimens with varying amounts of TiO2 (PEEK/0%, PEEK/20%, PEEK/>30%) were embedded, polished, air abraded (Al2O3, 50 µm, 0.4 MPa), conditioned using VL, and polymerized using either a halogen LCU (HAL-LCU) or a LED LCU (LED-LCU) for chairside or labside application, respectively. After thermocycling (5000×, 5/55 °C), TBS was measured, and fracture types were determined. Data was analyzed using a 2-way ANOVA followed by Tukey-HSD, Kruskal-Wallis H and Mann-Whitney U tests as well as a Chi²-test and a Ciba-Geigy table (p < 0.05). Globally, the light curing units, followed by PEEK composition, was shown to have the highest impact on TBS. The HAL-LCUs, compared to the LED-LCUs, resulted in a higher TBS for all PEEK compositions-without significant differences between chairside and labside units. Regarding the different PEEK compositions, PEEK/20%, compared to PEEK/0%, resulted in a higher TBS when both, HAL-LCUs or LED-LCUs were used for labside application. In comparison with PEEK/>30%, PEEK/20% resulted in a higher TBS after using HAL-LCU for labside application. No significant differences were found between PEEK/0% and PEEK/>30%. HAL-LCU with PEEK/20% for labside application showed a higher TBS than HAL-LCU with PEEK/20% for chairside application, whereas LED-LCU with PEEK/>30% for chairside application showed a higher TBS than LED-LCU with PEEK/>30% for labside application.

19.
Clin Oral Investig ; 21(4): 1183-1190, 2017 May.
Artigo em Inglês | MEDLINE | ID: mdl-27352903

RESUMO

OBJECTIVES: The study aims to characterise the curing behaviour of a light-curing luting composite (Variolink® Aesthetic LC, Ivoclar Vivadent) polymerised at different exposure times (10 s, 20 s) through different ceramics (IPS Empress CAD and IPS e.max CAD, Ivoclar Vivadent) and ceramic thicknesses (no ceramic, 0.5, 1, 1.5 and 2 mm). MATERIAL AND METHOD: Curing units' (Bluephase Style, Ivoclar Vivadent) variation in irradiance delivered up to 10-mm exposure distance as well as the incident and transmitted irradiance and radiant exposure up to 6-mm ceramic thickness were assessed on a laboratory-grade spectrometer. A total of 216 (18 groups, n = 12) thin and flat luting composite specimens of 500-µm thickness were prepared and stored after curing in a saturated vapour atmosphere for 24 h at 37 °C. Micro-mechanical properties (Vickers hardness, HV and indentation modulus, YHU) were determined by means of an automatic micro-hardness indenter. RESULTS: Within the study design, the radiant exposure received by the luting composite varied from 2.56 to 24.75 J/cm2, showing a high impact on the measured properties. Comparing the effect of the parameters exposure time, ceramic thickness and type, the highest influence on the micro-mechanical parameters was identified for exposure time, while this influence was stronger on HV (p < 0.001, η P2 = 0.452) than on YHU (p < 0.001, η P2 = 0.178). The influence of ceramic type was significant but low (η P2 = 0.161 on HV and 0.113 on YHU), while the influence of ceramic thickness was the lowest (η P2 = 0.04 and 0.05, respectively). CONCLUSIONS: Slightly higher irradiance values were transmitted through Empress CAD up to a ceramic thickness of 3 mm (p < 0.001), while being comparable with e.max for thicker slices. Differences in translucency between ceramics were reflected in the micro-mechanical properties of the luting composite. CLINICAL RELEVANCE: The radiant exposure reaching the luting composite is determined by the incident irradiance, exposure time, ceramic type and ceramic thickness. At the analysed incident irradiance, exposure time was the most consistent parameter affecting the micro-mechanical properties of the luting composite, and this effect was strongly reflected in the more translucent ceramic Empress CAD. Within the curing conditions, an exposure time of 20 s is recommended.


Assuntos
Silicatos de Alumínio/química , Cerâmica/química , Materiais Dentários/química , Porcelana Dentária/química , Cimentos de Resina/química , Dureza , Luz , Cura Luminosa de Adesivos Dentários , Teste de Materiais , Óptica e Fotônica , Polimerização , Propriedades de Superfície
20.
Odontology ; 104(3): 298-304, 2016 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-26762231

RESUMO

The aim of this study was to evaluate the influence of the physical assessment of different light-curing units from 55 dental offices on the irradiance and composite microhardness top/bottom ratio, and the influence of the radiometers for LED or QTH light sources on irradiance measurement. The irradiance of each light-curing unit was evaluated with two radiometers, either for LED or QTH light. A questionnaire regarding the type of source (LED or QTH), time of use, date of last maintenance and light-curing performance assessment applied. The physical assessments were evaluated regarding damage or debris on the light tip. For each light-curing unit, three composite specimens were made (diameter = 7 mm; thickness = 2 mm) with polymerizing time of 20 s, in order to perform the microhardness (Knoop) test. Data were analyzed by Kruskal-Wallis and Dunn test (α = 0.01). There was wide variation in irradiance (0-1000 mW/cm(2)). Approximately 50 % of the light-curing units presented radiation lower than 300 mW/cm(2); 10 % of light-curing units, especially those with LED source, presented values higher than 800 mW/cm(2), and 43 % of light-curing units worked with adequate irradiance between 301 and 800 mW/cm(2). In almost 60 % of cases, no maintenance of light-curing units was performed in a period of 3 to 10 years. The age of the light-curing units and the use of inadequate tips interfered negatively in irradiance. The data emphasize the importance of periodic maintenance of light-polymerizing, light-curing units.


Assuntos
Resinas Compostas/química , Lâmpadas de Polimerização Dentária , Brasil , Desenho de Equipamento , Análise de Falha de Equipamento , Dureza , Teste de Materiais , Processos Fotoquímicos , Doses de Radiação , Propriedades de Superfície , Inquéritos e Questionários
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