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Quality assurance of histamine analysis in fresh and canned fish.
Evangelista, Warlley P; Silva, Tarliane M; Guidi, Letícia R; Tette, Patrícia A S; Byrro, Ricardo M D; Santiago-Silva, Paula; Fernandes, Christian; Gloria, Maria Beatriz A.
Affiliation
  • Evangelista WP; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Silva TM; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Guidi LR; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Tette PA; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Byrro RM; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Santiago-Silva P; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.
  • Fernandes C; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil; Laboratório de Controle de Qualidade de Produtos Farmaceuticos e Cosmeticos, Faculdade de Farmácia, Universidade Federal de
  • Gloria MB; LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil. Electronic address: mbeatriz@ufmg.br.
Food Chem ; 211: 100-6, 2016 Nov 15.
Article in En | MEDLINE | ID: mdl-27283612
Histamine determination is relevant for fish safety, quality and trade. Recently a study by the European Union (EU) compared the Codex and the EU mandated methods for the analysis of histamine and observed that they underestimated and overestimated the results, respectively. To solve this problem, a simple and efficient procedure for the extraction and quantification of histamine by ion-pair HPLC method with post-column derivatization and fluorimetric detection is proposed. It was optimized and validated for the analysis of histamine in fish. The method attended the performance criteria established by Commission Decision 2002/657/CE. The method was also submitted to proficiency testing; uncertainty was calculated; and the stability of solutions and standards was investigated. There was no matrix effect. The LOD, LOQ, CCα and CCß were fit for the purpose. The method was successfully used in the analyses of freshwater fish and fresh and canned tuna.
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Histamine / Seafood / Food, Preserved Type of study: Prognostic_studies Limits: Animals Language: En Journal: Food Chem Year: 2016 Document type: Article Affiliation country: Brazil Country of publication: United kingdom
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Full text: 1 Collection: 01-internacional Database: MEDLINE Main subject: Histamine / Seafood / Food, Preserved Type of study: Prognostic_studies Limits: Animals Language: En Journal: Food Chem Year: 2016 Document type: Article Affiliation country: Brazil Country of publication: United kingdom