Multifrequency nonlinear Schrödinger equation.

The multifrequency character of nonlinearity dispersion is often dismissed because, in principle, it increases the computational load exceedingly rendering an impractical modeling and, typically, nonlinearities barely depend on frequency. Nonetheless, nonlinearity dispersion has recently enabled a solution to a long-standing challenge in optics. To explore the potential of this research avenue on solid theoretical grounds, we derive a propagation equation accounting for multifrequency nonlinearities rigorously that maintains the computational advantages of conventional models.

Nonlinearity measurement undergoing dispersion and loss.

Accurate knowledge of the nonlinear coefficient is extremely important to make reliable predictions about optical pulses propagating along waveguides. Nevertheless, determining this parameter when dispersion and loss are as important as nonlinear effects brings both theoretical and experimental challenges that have not yet been solved. A general method for measuring the nonlinear coefficient of waveguides under these demanding conditions is here derived and demonstrated experimentally in a kilometer-long standard silica fiber pumped close to 2 µm.

Denaturing for Nanoarchitectonics: Local and Periodic UV-Laser Photodeactivation of Protein Biolayers to Create Functional Patterns for Biosensing.

The nanostructuration of biolayers has become a paradigm for exploiting nanoscopic light-matter phenomena for biosensing, among other biomedical purposes. In this work, we present a photopatterning method to create periodic structures of biomacromolecules based on a local and periodic mild denaturation of protein biolayers mediated by UV-laser irradiation. These nanostructures are constituted by a periodic modulation of the protein activity, so they are free of topographic and compositional changes along the pattern. Herein, we introduce the approach, explore the patterning parameters, characterize the resulting structures, and assess their overall homogeneity. This UV-based patterning principle has proven to be an easy, cost-effective, and fast way to fabricate large areas of homogeneous one-dimensional protein patterns (2 min, 15 × 1.2 mm, relative standard deviation ≃ 16%). This work also investigates the implementation of these protein patterns as transducers for diffractive biosensing. Using a model immunoassay, these patterns have demonstrated negligible signal contributions from non-specific bindings and comparable experimental limits of detection in buffer media and in human serum (53 and 36 ng·mL-1 of unlabeled IgG, respectively).

Recent Advances in Forward Brillouin Scattering: Sensor Applications.

In-fiber opto-mechanics based on forward Brillouin scattering has received increasing attention because it enables sensing the surrounding of the optical fiber. Optical fiber transverse acoustic resonances are sensitive to both the inner properties of the optical fiber and the external medium. A particularly efficient pump and probe technique-assisted by a fiber grating-can be exploited for the development of point sensors of only a few centimeters in length. When measuring the acoustic resonances, this technique provides the narrowest reported linewidths and a signal-to-noise ratio better than 40 dB. The longitudinal and transverse acoustic velocities-normalized with the fiber radius-can be determined with a relative error lower than 10-4, exploiting the derivation of accurate asymptotic expressions for the resonant frequencies. Using this technique, the Poisson's ratio of an optical fiber and its temperature dependence have been measured, reducing the relative error by a factor of 100 with respect to previously reported values. Using a single-point sensor, discriminative measurements of strain and temperature can be performed, achieving detection limits of ±25 µÎµ and ±0.2 °C. These results show the potential of this approach for the development of point sensors, which can be easily wavelength-multiplexed.

Application of WGM Resonances to the Measurement of the Temperature Increment of Ho and Ho-Yb Doped Optical Fibers Pumped at 1125 and 975 nm.

Optical fiber characterization using whispering gallery mode resonances of the fiber itself has been demonstrated to be a powerful technique. In this work, we exploit the thermal sensitivity of whispering gallery mode resonances to characterize the pump-induced temperature increment in holmium doped and holmium-ytterbium codoped optical fibers. The technique relies on the measurement of the resonances' wavelength shift due to temperature variation as a function of the pump power. Holmium doped fibers were pumped to the second excited level 5I6 of the Ho3+ ion using a laser diode at 1125 nm and ytterbium-holmium codoped fibers to the 2F5/2 level of the Yb3+ ion by a laser diode at 975 nm. Our results demonstrate that pumping ytterbium-holmium codoped fibers at 975 nm results in dramatic thermal effects, producing a temperature increment two orders higher than that observed in holmium doped fibers pumped with a 1125 nm laser diode.

BIO bragg gratings on microfibers for label-free biosensing.

Discovering nanoscale phenomena to sense biorecognition events introduces new perspectives to exploit nanoscience and nanotechnology for bioanalytical purposes. Here we present Bio Bragg Gratings (BBGs), a novel biosensing approach that consists of diffractive structures of protein bioreceptors patterned on the surface of optical waveguides, and tailored to transduce the magnitude of biorecognition assays into the intensity of single peaks in the reflection spectrum. This work addresses the design, fabrication, and optimization of this system by both theoretical and experimental studies to explore the fundamental physicochemical parameters involved. Functional biomolecular gratings are fabricated by microcontact printing on the surface of tapered optical microfibers, and their structural features were characterized. The transduction principle is experimentally demonstrated, and its quantitative bioanalytical prospects are assessed in a representative immunoassay, based on patterned protein probes and selective IgG targets, in label-free conditions. This biosensing system involves appealing perspectives to avoid unwanted signal contributions from non-specific binding, herein investigated in human serum samples. The work also proves how the optical response of the system can be easily tuned, and it provides insights into the relevance of this feature to conceive multiplexed BBG systems capable to perform multiple label-free biorecognition assays in a single device.

Monitoring the Growth of a Microbubble Generated Photothermally onto an Optical Fiber by Means Fabry-Perot Interferometry.

In the present paper, we show the experimental measurement of the growth of a microbubble created on the tip of a single mode optical fiber, in which zinc nanoparticles were photodeposited on its core by using a single laser source to carry out both the generation of the microbubble by photothermal effect and the monitoring of the microbubble diameter. The photodeposition technique, as well as the formation of the microbubble, was carried out by using a single-mode pigtailed laser diode with emission at a wavelength of 658 nm. The microbubble's growth was analyzed in the time domain by the analysis of the Fabry-Perot cavity, whose diameter was calculated with the number of interference fringes visualized in an oscilloscope. The results obtained with this technique were compared with images obtained from a CCD camera, in order to verify the diameter of the microbubble. Therefore, by counting the interference fringes, it was possible to quantify the temporal evolution of the microbubble. As a practical demonstration, we proposed a vibrometer sensor using microbubbles with sizes of 83 and 175 µm as a Fabry-Perot cavity; through the time period of a full oscillation cycle of an interferogram observed in the oscilloscope, it was possible to know the frequency vibration (500 and 1500 Hz) for a cuvette where the microbubble was created.

Measurement of the soliton number in guiding media through continuum generation.

No general approach is available yet to measure directly the ratio between chromatic dispersion and the nonlinear coefficient, and hence the soliton number for a given optical pulse, in an arbitrary guiding medium. Here we solve this problem using continuum generation. We experimentally demonstrate our method in polarization-maintaining and single-mode fibers with positive and negative chromatic dispersion. Our technique also offers new opportunities to determine the chromatic dispersion of guiding media over a broad spectral range while pumping at a fixed wavelength.

High-speed and high-resolution interrogation of FBG sensors using wavelength-to-time mapping and Gaussian filters.

In this work we report a novel intensity-based technique for simultaneous high-speed and high-resolution interrogation of fiber Bragg grating (FBG) sensors. The method uses a couple of intensity Gaussian filters and the dispersion-induced wavelength-to-time mapping effect. The Bragg wavelength is retrieved by means of the amplitude comparison between the two filtered grating spectrums, which are mapped into a time-domain waveform. In this way, measurement distortions arising from residual power due to the grating sidelobes are completely avoided, and the wavelength measurement range is considerably extended with respect to the previously proposed schemes. We present the mathematical background for the interrogation of FBGs with an arbitrary bandwidth. In our proof-of-concept experiments, we achieved sensitivities of ∼20 pm with ultra-fast rates up to 264 MHz.

Ytterbium-doped fiber laser as pulsed source of narrowband amplified spontaneous emission.

We report random noise pulsed regime of an ytterbium-doped fiber laser arranged in common Fabry-Perot configuration. We show that the laser output obeys the photon statistics inherent to narrowband amplified spontaneous emission and that the noise pulsing is properly addressed in terms of probability density and autocorrelation functions. Our novel approach reveals, in particular, that the regime's coherence time dramatically shortens, from few ns to tens ps, with increasing laser power.